Modification HKUST-1 as a catalyst for the reduction of 4-nitrophenol

Bui Thi Thanh Ha; Le Van Duong; Le Ngoc Duong; Ta Ngoc Hung; Nguyen Le Anh; Ta Ngoc Don

doi:10.51316/jca.2021.065

Authors

Bui Thi Thanh Ha Hanoi University of Pharmacy Author
Le Van Duong School of Chemical Engineering, Hanoi University of Science and Technology, Vietnam Author
Le Ngoc Duong Hanoi College of Medicine and Pharmacy Author
Ta Ngoc Hung Deakin University, Australia Author
Nguyen Le Anh High School for the Gifted, Hanoi National University of Education Author
Ta Ngoc Don School of Chemical Engineering, Hanoi University of Science and Technology, Vietnam Author

DOI:

https://doi.org/10.51316/jca.2021.065

Keywords:

HKUST-1, MOFS-199, Metal Organic Frameworks (MOFs), 4-nitrophenol, 4-aminophenol, paracetamol

Abstract

HKUST-1 (MOF-199), a metal-organic framework material is synthesized from Cu(OH)₂ and modified by Pt. The prepared catalysts were used to reduce 4-nitrophenol (4-NP) into 4-aminophenol (4-AP). Featured results of the catalysts by XRD, SEM, TEM, FTIR, BET, DTA/TGA... showed that metal modified process with reduced agent ethylene glycol had high efficiency, with modified yield up to 90 %. Under our experimental conditions, the catalysts based HKUST-1, containing Pt had high efficiency; conversion was greater than 93 % in reduced reaction of 4-NP. Thus, the catalyst sample contained 2% Pt was the most suitable for the reduction with conversion gained 99,4 % after 250s.

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