Effect of silica in ordered mesoporous carbon based catalyst derived from rice husk on its characterizations and activity in synthesis of biolubricant from castor oil
Abstract
The report published study on effect of silica in rice husk affecting preparation, characterizations and application ability of ordered mesoporous carbon based catalyst. The catalysts were prepared through condensation-evaporation method using sulfonated biochar as precursor. Silica content in the biochar was removed, and the catalysts were prepared in two cases: using the sufonated biochar before and after the silica removal. These catalysts were also applied in conversion of castor oil to ester based biolubricant for their activity comparison. The results showed that silica content in the rice husk played a very minor role in the structure, characteristics and activity of the ordered mesoporous carbon based catalyst in the biolubricant synthesis. Some techniques were applied in the study including SAXRD, WAXRD, FT-IR, NH3-TPD and GC-MS.
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