Using XRD to study the factors affecting the synthesis of nano-ZIF-94 from zinc chloride

Hải Trịnh; Hương Phạm; Dương Lê; Huy Tạ; Anh Hà; Quỳnh Lê; Quang Nguyễn; Vỹ Trần; Đôn Tạ

doi:10.62239/jca.2025.047

Authors

Trinh Thi Hai Hanoi University of Industry
Pham Thi Mai Huong Hanoi University of Industry
Le Van Duong School of Chemistry and Life Sciences, Hanoi University of Science and Technology, 1 Dai Co Viet, Hanoi, Vietnam
Ta Ngoc Thien Huy Kien Giang University
Ha Thi Lan Anh Food Industrial College, Viet Tri, Phu Tho
Le Thi Nhu Quynh Pham Van Dong University
Nguyen Viet Quang Military Petroleum Technical Institute
Trần Anh Vỹ Nguyen Tat Thanh University
Ta Ngoc Don School of Chemistry and Life Sciences, Hanoi University of Science and Technology, 1 Dai Co Viet, Hanoi, Vietnam

DOI:

https://doi.org/10.62239/jca.2025.047

Keywords:

ZIF-94, SIM-1, zinc chloride, synthesis, characterization

Abstract

ZIF-94 was successfully synthesized from zinc chloride at atmospheric pressure. The factors affecting the synthesis of ZIF-94 were studied in detail.

Using X-ray diffraction (XRD) to evaluate the crystallization process of nano-ZIF-94 by changing the solvent, additives, solvent content, additives content, and linker content. The factors of temperature and reaction time were also discussed. The crystallinity, crystal size of nano-ZIF-94 formed and the yield of nano-ZIF-94 were also mentioned. This is the first paper to present the results of the synthesis of nano-ZIF-94 from zinc chloride.

Downloads

Download data is not yet available.

References

W. Morris, N. He, K.G. Ray, P. Klonowski, H. Furukawa, I.N. Daniels, Y.A. Houndonougbo, M. Asta, O.M. Yaghi, B.B. Laird, J. Phys. Chem. C, 116(45) (2012) 24084–24090. https://doi.org/10.1021/jp307170a

S. Aguado, J. Canivet, D. Farrusseng, Chem. Commun., 46(42) (2010) 7999–8001. https://doi.org/10.1039/C0CC02045A

N.K.D. Hong, T.N. Don, N.T. Hung, J. Appl. Chem., 6(1) (2017) 50–68. https://www.researchgate.net/publication/312932923

T.N. Don, V.D. Thang, P.T. Huyen, P.M. Hao, N.K.D. Hong, Stud. Surf. Sci. Catal., 159 (2006) 197–200. https://doi.org/10.1016/S0167-2991(06)81567-3

X.-C. Huang, Y.-Y. Lin, J.-P. Zhang, X.-M. Chen, Angew. Chem. Int. Ed., 45(10) (2006) 1557–1559. https://doi.org/10.1002/anie.200503778

N.K.D. Hong, D.T. Ngo, N.L.T. Nga, T.N. Don, J. Porous Mater., 24(2) (2017) 559–566. https://doi.org/10.1007/s10934-016-0291-z

N.K.D. Hong, T.N. Don, G. Sankar, R.A. Catlow, Catal. Commun., 25 (2012) 125–129. https://doi.org/10.1016/j.catcom.2011.11.016

Q. Shi, J. Wang, H. Shang, H. Bai, Y. Zhao, J. Yang, J. Dong, J. Li, Sep. Purif. Technol., 230 (2020) 115850. https://doi.org/10.1016/j.seppur.2019.115850

M. Li, J. Liu, S. Deng, Q. Liu, N. Qi, Z. Chen, ACS Appl. Energy Mater., 4(8) (2021) 7983–7991. https://doi.org/10.1021/acsaem.1c01297

Q. Wang, Y. Chen, P. Liu, Y. Wang, J. Yang, J. Li, L. Li, Molecules, 27(17) (2022) 5608. https://doi.org/10.3390/molecules27175608

B.C. Marepally, C. Ampelli, C. Genovese, T. Saboo, S. Perathoner, F.M. Wisser, L. Veyre, J. Canivet, E.A. Quadrelli, G. Centi, ChemSusChem, 10(22) (2017) 4442–4446. https://doi.org/10.1002/cssc.201701506

S. Aguado, S. El-Jamal, F. Meunier, J. Canivet, D. Farrusseng, Chem. Commun., 52(45) (2016) 7161–7163. https://doi.org/10.1039/C6CC03096C

T.N. Don, N.T.H. Phuong, N.T.M. Thu, N.T.T. Huyen, T.N.T. Huy, N.V. Thanh, D. Mo, N.T. Nghia, P.T.M. Huong, N.T. Linh, H.T.L. Anh, B.T.T. Ha, T.A. Vy, T.T. Hai, Vietnam J. Catal. Adsorpt., 12(4) (2023) 1–18. https://doi.org/10.62239/jca.2023.060

T.T. Hai, T.T.T. Vy, L.N. Duong, N.T. Thao, P.T.M. Huong, T.N.T. Huy, L.N.T. Long, N.T.M. Thu, L.V. Duong, T.N. Don, Vietnam J. Catal. Adsorpt., 14(2) (2025) 38–42. https://doi.org/10.62239/jca.2025.022

T.T. Hai, P.T.M. Huong, T.N.T. Huy, D.N. Lam, P.Q. Huy, N.S. Tuan, N.X. Thong, N.H. Giang, L.V. Duong, T.N. Don, Vietnam J. Catal. Adsorpt., 13(4) (2024) 79–84. https://doi.org/10.62239/jca.2024.078

V.A. Tran, V.D. Doan, V.T. Le, T.Q. Nguyen, T.N. Don, V. Vien, N.T. Luan, G.N.L. Vo, Ind. Eng. Chem. Res., 62(11) (2023) 4738–4753. https://doi.org/10.1021/acs.iecr.2c04399

L. Paseta, M. Malankowska, C. Téllez, J. Coronas, Mater. Chem. Phys., 295 (2023) 127039. https://doi.org/10.1016/j.matchemphys.2022.127039

T.N. Don, L.V. Duong, N.T.H. Phuong, N.T.T. Huyen, T.N.T. Huy, D. Mo, B.T.T. Ha, T.A. Vy, Can. J. Chem. Eng., 103(1) (2025) 311–322. https://doi.org/10.1002/cjce.25382

M.R. Hasan, L. Paseta, M. Malankowska, C. Téllez, J. Coronas, Adv. Sustainable Syst., 6 (2022) 2100317. https://doi.org/10.1002/adsu.202100317

Mercury – The Cambridge Crystallographic Data Centre (CCDC), truy cập 09 May 2020. https://www.ccdc.cam.ac.uk/solutions/csdsystem/components/mercury/

Structures – CCDC, truy cập 09 May 2020. https://www.ccdc.cam.ac.uk/structures/Search?Compound=ZIF-8&DatabaseToSearch=Published