Preparation of nano-ZIF-90 from zinc acetate dihydrate

Ta Ngoc Thien Huy; Lê Huyền Trâm; Nguyễn Văn Thành; Trần Thị Thảo Vy; Lê Ngọc Dương; Nhữ Thị Thảo; Bùi Thị Thanh Hà; Ninh Thị Phương; Lê Văn Dương; Ta Ngoc Don

doi:10.62239/jca.2025.018

Authors

Ta Ngoc Thien Huy Kien Giang University | School of Chemistry and Life Sciences, Hanoi University of Science and Technology
Le Huyen Tram School of Chemistry and Life Sciences, Hanoi University of Science and Technology
Nguyen Van Thanh Kien Giang University
Tran Thi Thao Vy Nha Trang University
Le Ngoc Duong Hanoi Dong Do International University
Nhu Thi Thao School of Chemistry and Life Sciences, Hanoi University of Science and Technology, 1 Dai Co Viet, Hanoi, VIETNAM
Bui Thi Thanh Ha Hanoi University of Pharmacy
Ninh Thi Phuong School of Chemistry and Life Sciences, Hanoi University of Science and Technology
Le Van Duong School of Chemistry and Life Sciences, Hanoi University of Science and Technology, 1 Dai Co Viet, Hanoi, VIETNAM
Ta Ngoc Don School of Chemistry and Life Sciences, Hanoi University of Science and Technology, 1 Dai Co Viet, Hanoi, VIETNAM

DOI:

https://doi.org/10.62239/jca.2025.018

Keywords:

ZIF-90, zinc acetate dihydrate, synthesis, characterization

Abstract

Nanometer-sized ZIF-90 has been preparatied from zinc acetate dihydrate with high yield. XRD, F-TIR, SEM, TEM, BET, DTA methods were used to characterize the research samples. The results have shown that the formed ZIF-90 has crystallinity of 100 %, BET specific surface reaches 1,051 m²/g, of which the external surface reaches 292 m²/g, total capillary volume reaches 0.472 cm³/g, average crystal size of 38 nm (according to SEM), heat stable up to 285 ^oC and efficiency of 78.2 %.

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