Synthesis and evaluation of catalytic activities in rhodamine B degraded reaction by H2O2 of MIL-53(Al) dopping with iron

Huynh Tuan Anh; Nguyen Huu Nghi; Pham Thi Hong Duyen; Pham Dinh Du

doi:10.51316/jca.2022.026

Authors

Huynh Tuan Anh Dong Thap University, 783 Pham Huu Lau, Cao Lanh city, Dong Thap
Nguyen Huu Nghi Dong Thap University, 783 Pham Huu Lau, Cao Lanh city, Dong Thap
Pham Thi Hong Duyen Thu Dau Mot University
Pham Dinh Du Thu Dau Mot University

DOI:

https://doi.org/10.51316/jca.2022.026

Keywords:

Fe-MIL-53(Al), Metal-organic, framework, Rhodamine B, Degradation

Abstract

In the present study, MIL-53(Al) metal-organic framework material dopping with iron (denoted as Fe-MIL-53(Al)) had been synthesized and applied as a catalyst to degrade rhodamine B (RB) in aqueous solution by H₂O₂. The obtained materials were characterized using X-ray diffraction (XRD), thermogravimetry analysis (TG), transmission electron microscopy (TEM), and energy dispersive X-ray (EDX). The influence of iron content on the structure of MIL-53(Al) and treated temperature of Fe-MIL-53(Al) were investigated. The results showed that the obtained Fe-MIL-53(Al), which was synthesized at mole ratio of Fe/Al = 1/9, had high catalytic activity for RB oxidation reaction by H₂O₂, RB degradation efficiency was 92%, and achieved 100% under UV radiation ([RB] = 10 mg/L). The treatment at 280 ºC had almost no effect on the structure of the material, but also slightly enhanced the catalytic activity.

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